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- W2162230303 abstract "A method for the synthesis of β3-amino acids starting from α-amino acids is described. This conversion can be effected by an eight-step procedure which involves the transformation of the carboxylic group into an alkyne followed by a selenium-mediated conversion of the carbon–carbon triple bond to a Se-phenyl selenocarboxylate intermediate. The reactive Se-phenyl selenocarboxylate intermediates can be trapped with water, alcohols or the amine of an amino acid derivative to give β3-amino acids, β3-amino esters or mixed peptides, respectively. The whole transformations of the carboxylic group into an alkyne and of the alkyne group into β3-amino acids may not require purification of the intermediate products but a work-up and isolation procedure of crude materials." @default.
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- W2162230303 date "2010-08-01" @default.
- W2162230303 modified "2023-10-17" @default.
- W2162230303 title "A reasonably stereospecific multistep conversion of Boc-protected α-amino acids to Phth-protected β3-amino acids" @default.
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- W2162230303 doi "https://doi.org/10.1016/j.tetlet.2010.05.143" @default.
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