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• W2162510562 abstract "Four silicate glasses were prepared by the fusion of about 1 kg powder each of a basalt, syenite, soil and andesite to provide reference materials of natural composition for microanalytical work. These glasses are referred to as ‘Chinese Geological Standard Glasses’ (CGSG) -1, -2, -4 and -5. Micro and bulk analyses indicated that the glasses are well homogenised with respect to major and trace elements. Some siderophile/chalcophile elements (e.g., Sn, Pt, Pb) may be heterogeneously distributed in CGSG-5. This paper provides the first analytical data for the CGSG reference glasses using a variety of analytical techniques (wet chemistry, XRF, EPMA, ICP-AES, ICP-MS, LA-ICP-MS) performed in nine laboratories. Most data agree within uncertainty limits of the analytical techniques used. Discrepancies in the data for some siderophile/chalcophile elements exist, mainly because of possible heterogeneities of these elements in the glasses and/or analytical problems. From the analytical data, preliminary reference and information values for fifty-five elements were calculated. The analytical uncertainties [2 relative standard error (RSE)] were estimated to be between about 1% and 20%. Quatre verres silicatés ont été préparés par fusion d’environ 1 kg de poudre respectivement de basalte, de syénite, de sol et d’andésite pour fournir des matériaux naturels de référence pour la microanalyse. Ces verres sont dénommés ‘Verres Standard Géologiques Chinois’ (CGSG) -1, -2, -4 et -5. La microanalyse et l’analyse globale ont indiqué que les verres sont très homogènes en termes d’éléments majeurs et traces. Certains éléments sidérophiles et chalcophiles (par exemple, Sn, Pt, Pb) peuvent être distribués de façon hétérogène dans le verre CGSG-5. Cet article fournit les premières données pour les verres de référence CGSG en utilisant une variété de techniques d’analyse (chimie par voie humide, XRF, EPMA, ICP-AES, ICP-MS, LA-ICP-MS) réparties dans neuf laboratoires. La plupart des données sont dans les limites d’incertitude des techniques analytiques utilisées. Des écarts dans les données pour certains éléments sidérophiles et chalcophiles existent, principalement en raison des hétérogénéités possibles de distribution de ces éléments dans les verres et/ou de problèmes analytiques. A partir des données, des valeurs préliminaires de référence et des valeurs d’information ont été calculés pour cinquante-cinq éléments. Les incertitudes d’analyse (2 RSE) ont été estimées être comprises entre 1 et 20%." @default.
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• W2162510562 date "2010-12-06" @default.
• W2162510562 modified "2023-10-14" @default.
• W2162510562 title "Preliminary Characterisation of New Reference Materials for Microanalysis: Chinese Geological Standard Glasses CGSG-1, CGSG-2, CGSG-4 and CGSG-5" @default.
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• W2162510562 doi "https://doi.org/10.1111/j.1751-908x.2010.00097.x" @default.
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