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- W2162764170 abstract "A family of well-defined FeII complexes of the type {BnN(N-CH2(CH2)n-N′-tert-butyl-imidazole-2-ylidene)2}FeCl2 (Bn = benzyl; n = 1 (1) or 2 (2)), {BnN(N-CH2(CH2)n-N′-methylbenzimidazole-2-ylidene)2}FeCl2 (n = 1 (3) or 2 (4)) and {BnN(N-CH2CH2CH2-N′-methylbenzimidazole-2-ylidene)2}FeBr2 (5) has been synthesized. These complexes are rare examples of Fe species supported by bidentate NHC ligands. Complexes 2, 3, 4 and 5 were characterized by X-ray crystallography and in all cases a distorted tetrahedral geometry is observed around the Fe center. The magnetic data is consistent with the complexes containing non interacting high spin FeII centers (S = 2) and indicates that a large zero-field splitting (D) is present. The new complexes are highly active pre-catalysts for the homo-coupling of Grignard reagents." @default.
- W2162764170 created "2016-06-24" @default.
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- W2162764170 date "2013-01-01" @default.
- W2162764170 modified "2023-10-16" @default.
- W2162764170 title "Synthesis and catalytic activity of iron complexes with bidentate NHC ligands" @default.
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- W2162764170 doi "https://doi.org/10.1039/c3dt32551b" @default.
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