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- W2163721503 abstract "Abstract Negishi cross-coupling of the silyl-protected 3-bromoenol of 1,2-cyclopentanedione with primary and secondary alkylzinc reagents using Pd-catalysts affords 3-alkyl substituted 1,2-cyclopentanediones in good yield. The method was applied to obtain 3-methylalkoxycarbonyl- and 3(2-Boc-aminoethyl)-alkoxycarbonyl-1,2-cyclopentanediones—homocitric and lycoperdic acid precursors. Homocitric and lycoperdic acids were synthesized using asymmetric oxidation with the Ti(OiPr)4/tartaric ester/tBuOOH complex in two steps from the obtained precursors." @default.
- W2163721503 created "2016-06-24" @default.
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- W2163721503 date "2015-12-01" @default.
- W2163721503 modified "2023-10-14" @default.
- W2163721503 title "3-Alkyl-1,2-cyclopentanediones by Negishi cross-coupling of a 3-bromo-1,2-cyclopentanedione silyl enol ether with alkylzinc reagents: an approach to 2-substituted carboxylic acid γ-lactones, homocitric and lycoperdic acids" @default.
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- W2163721503 doi "https://doi.org/10.1016/j.tet.2015.10.014" @default.
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