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• W2163738976 abstract "Abstract The chemisorbates formed from ammonia-containing alkaline electrolyte on gold and palladium electrodes have been identified using surface-enhanced Raman spectroscopy (SERS). On gold, a potential-dependent band at ca. 365– 385 cm −1 is observed, consistent with the metal–nitrogen stretch for molecular adsorbed ammonia on the basis of the frequency redshift observed upon deuteration. A similar feature is also observed on palladium, at 440– 455 cm −1 , again consistent with chemisorbed ammonia on the basis of the H/D shift. On palladium, but not on gold, however, transfer of the electrode to ammonia-free electrolyte yielded a vibrational band at 455– 465 cm −1 . The near-zero H/D frequency shift obtained for this irreversibly adsorbed component indicates the formation of chemisorbed atomic nitrogen on palladium. This finding is discussed in terms of the mechanism for ammonia electro-oxidation." @default.
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• W2163738976 date "2001-06-01" @default.
• W2163738976 modified "2023-09-26" @default.
• W2163738976 title "The nature of chemisorbates formed from ammonia on gold and palladium electrodes as discerned from surface-enhanced Raman spectroscopy" @default.
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• W2163738976 doi "https://doi.org/10.1016/s1388-2481(01)00156-4" @default.
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