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- W2164043695 abstract "Millimeter-sized hydroxyapatite (HA) single crystals were synthesized from chlorapatite (ClAp) crystals via the ionic exchange of Cl− for OH− at high temperature. X-ray diffraction, Fourier-transform infrared spectroscopy, and chloride content measurements were used to follow the progress of this conversion, and to assess the effect of the experimental conditions (temperature, time, and atmosphere). Cl−→OH− exchange took place homogeneously and was enhanced by firing in wet air. After firing at 1425°C for 2 h 92% of the Cl− ions were exchanged by OH− while maintaining crystal integrity. Temperatures above 1450°C damaged the surface of the crystals, destroying the hexagonal habit at 1500°C. The composition of these apatite crystals was close to bone mineral content. Their nanoindentation hardness (8.7 ± 1.0 GPa) and elastic nanoindentation modulus (120 ± 10 GPa) were similar to those of the starting ClAp (6.6 ± 1.5 GPa, and 110 ± 15 GPa, respectively). However, their average flexural strength was ~25% lower due to the formation of defects during the thermal treatments." @default.
- W2164043695 created "2016-06-24" @default.
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- W2164043695 date "2013-03-01" @default.
- W2164043695 modified "2023-10-18" @default.
- W2164043695 title "Synthesis and Optimization of the Production of Millimeter-Sized Hydroxyapatite Single Crystals by Cl<sup>−</sup> -OH<sup>−</sup> Ion Exchange" @default.
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- W2164043695 doi "https://doi.org/10.1111/jace.12199" @default.
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