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- W2164118798 abstract "An integrated suite of synthesis and characterisation techniques that includes synchrotron-based single crystal, powder X-ray diffraction, nuclear magnetic resonance and electron diffraction have been employed to uncover two new distinct structures in the CaxBa2−xP2O7 polymorphic phosphate system. These materials have particular relevance for their application as both biomaterials and phosphors. Calcium barium pyrophosphate, CaBaP2O7, was shown by a combination of spectroscopic and diffraction techniques to have two polymorphs distinct in structure from all of the five previously reported polymorphs of Ca, Sr and Ba pyrophosphate. A high temperature polymorph HT-CaBaP2O7 prepared at 1200 °C is orthorhombic, of space group P212121 with a = 13.0494 Å, b = 8.9677 Å, c = 5.5444 Å. A low temperature polymorph LT-CaBaP2O7, prepared below 1000 °C, is monoclinic with space group P21/c and dimensions a = 12.065 Å, b = 10.582 Å, c = 9.515 Å, β = 94.609°." @default.
- W2164118798 created "2016-06-24" @default.
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- W2164118798 date "2012-01-01" @default.
- W2164118798 modified "2023-10-18" @default.
- W2164118798 title "A simple route to full structural analysis of biophosphates and their application to materials discovery" @default.
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- W2164118798 doi "https://doi.org/10.1039/c2dt00023g" @default.
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