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• W2164800544 endingPage "1577" @default.
• W2164800544 startingPage "1570" @default.
• W2164800544 abstract "We report the first studies on the reaction between an HNO donor compound and vitamin B12 complexes. Kinetic and mechanistic studies have been carried out on the reaction between the vitamin B12 derivative aquacobalamin (H2OCbl+/HOCbl; pKa = 7.8) and the HNO donor Angeli’s salt. Studies were carried out with aquacobalamin in excess, since nitrite also reacts with aquacobalamin to form nitrocobalamin (NO2Cbl). At pH <9.90 aquacobalamin reacts directly with the monoprotonated form of Angeli’s salt, HN2O3–, to form nitroxylcobalamin (NO–-Cbl(III); NOCbl) and nitrite. At pH >10.80 the reaction instead switches predominantly to a mechanism in which spontaneous decomposition of Angeli’s salt to give HNO and nitrite becomes the rate-determining step, followed by the rapid reaction between aquacobalamin and HNO/NO– to again give NOCbl. Both reactions proceed with a 1:1 stoichiometry and formation of nitrite is confirmed using the Griess assay." @default.
• W2164800544 created "2016-06-24" @default.
• W2164800544 creator A5071522367 @default.
• W2164800544 creator A5073609279 @default.
• W2164800544 creator A5091484015 @default.
• W2164800544 date "2014-01-17" @default.
• W2164800544 modified "2023-09-25" @default.
• W2164800544 title "Kinetic and Mechanistic Studies on the Reaction of the Vitamin B₁₂ Complex Aquacobalamin with the HNO Donor Angeli’s Salt: Angeli’s Salt and HNO React with Aquacobalamin" @default.
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• W2164800544 doi "https://doi.org/10.1021/ic402613z" @default.
• W2164800544 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/24437629" @default.
• W2164800544 hasPublicationYear "2014" @default.
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