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• W2165112604 abstract "In this study, the steroid hormone levels in river and tap water samples were determined by using a novel dispersive liquid-liquid microextraction method based on the solidification of a floating organic drop (DLLME-SFO). Several parameters were optimized, including the type and volume of the extraction and dispersive solvents, extraction time, and salt effect. DLLME-SFO is a fast, cheap, and easy-to-use method for detecting trace levels of samples. Most importantly, this method uses less-toxic solvent. The correlation coefficient of the calibration curve was higher than 0.9991. The linear range was from 5 to 1000 microg L(-1). The spiked environmental water samples were analyzed using DLLME-SFO. The relative recoveries ranged from 87% to 116% for river water (which was spiked with 4 microg L(-1) for E1, 3 microg L(-1) for E2, 4 microg L(-1) for EE2 and 9 microg L(-1) for E3) and 89% to 102% for tap water (which was spiked with 6 microg L(-1) for E1, 5 microg L(-1) for E2, 6 microg L(-1) for EE2 and 10 microg L(-1) for E3). The detection limits of the method ranged from 0.8 to 2.7 microg L(-1) for spiked river water and 1.4 to 3.1 microg L(-1) for spiked tap water. The methods precision ranged from 8% to 14% for spiked river water and 7% to 14% for spiked tap water." @default.
• W2165112604 created "2016-06-24" @default.
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• W2165112604 date "2010-03-01" @default.
• W2165112604 modified "2023-10-06" @default.
• W2165112604 title "Determination of the steroid hormone levels in water samples by dispersive liquid–liquid microextraction with solidification of a floating organic drop followed by high-performance liquid chromatography" @default.
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• W2165112604 doi "https://doi.org/10.1016/j.aca.2010.01.003" @default.
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