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- W2165163207 abstract "Five different methods were used to prepare the Ni-Mo oxide precursors including sol-gel, rotary evaporation-microwave drying, co-precipitation, impregnation, and mechanical mixing. Ni-Mo nitride catalysts have been synthesized by temperature-programmed nitration of the oxide precursors in a flow of H2 and N2. The structure and physico-chemical properties of the Ni-Mo oxide precursors and their corresponding nitride catalysts were determined by X-ray diffraction, total nitrogen content analysis, X-ray photoelectron spectroscopy and H2 temperature-programmed reduction, and their catalytic performance for propane ammoxidation was also tested. The catalytic activity and selectivity towards the formation of acrylonitrile over the Ni-Mo nitride catalysts are strongly dependent on the preparation methods for the oxide precursors. The N species in the Ni-Mo nitrides and their mobility and reactivity affect the selectivity for acrylonitrile. The Ni-Mo nitride prepared by co-precipitation, with the largest amount and more reactive N species, exhibited the highest catalytic activity and selectivity for acrylonitrile." @default.
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- W2165163207 date "2014-03-01" @default.
- W2165163207 modified "2023-10-16" @default.
- W2165163207 title "Ni-Mo nitride catalysts: Synthesis and application in the ammoxidation of propane" @default.
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- W2165163207 doi "https://doi.org/10.1016/s1872-2067(14)60015-2" @default.
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