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- W2166248032 abstract "Abstract Tin‐doped indium oxide electrodes are fabricated and employed in a dual‐plate microtrench geometry with the inter‐electrode gap controlling the mass transport conditions in generator‐collector mode. Electrodes are fabricated with 2–50 µm gap sizes and variable trench depths by controlling assembly parameters. Non‐ideal behaviour is observed for three aqueous redox systems: Ru(bpy) ${{{3+/2+hfill atop 3hfill}}}$ , 1,1′‐ferrocenedimethanol and Ru(NH 3 ) ${{{3+/2+hfill atop 6hfill}}}$ . Under fast mass transport conditions, the former two systems exhibit slower oxidation features. For Ru(NH 3 ) ${{{3+/2+hfill atop 6hfill}}}$ , non‐steady‐state behaviour is observed due to irreversible (EC irrev ′) consumption of oxygen in the microtrench. A mechanism leading to hydrogen peroxide formation via superoxide in Ru(NH 3 ) ${{{2+hfill atop 6hfill}}}$ solution is proposed. Under optimised conditions all three redox systems provide reliable trench depth calibration information." @default.
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- W2166248032 date "2015-03-06" @default.
- W2166248032 modified "2023-10-16" @default.
- W2166248032 title "ITO-ITO Dual-Plate Microgap Electrodes: E and EC′ Generator-Collector Processes" @default.
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