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- W2167121036 abstract "Nano-scaled lead-free perovskite powders (50–100 nm) with a composition of (Na0.52K0.4425)(Nb0.8825Sb0.08)O3-0.0375LiTaO3 (NKNS-3.75LT) have been synthesized via a modified low-cost citrate sol–gel route, in which Nb2O5 and Ta2O5 were transformed into stable and soluble chelate complexes to replace costly metal alkoxides. The thermal decomposition process and structural transformation behavior of the as-prepared xerogel was investigated by means of thermo-gravitometry and differential scanning calorimetry, X-ray diffractometry and Fourier-transform infrared spectrometry. The results indicated that the ideal crystallization of the NKNS-3.75LT powder with a single perovskite structure occurs at 500–600 °C, significantly lower than that for a conventional mixed-oxide route. Transmission electron microscopy observation showed that the crystalline powder has particle sizes in the range of 30–100 nm and exhibits polyhedron-like morphology, probably resulting in a specific grain growth behavior upon densification. The sol–gel derived NKNS-3.75LT ceramics sintered at 1090 °C exhibit excellent piezoelectric properties of d33 ∼418 pC/N and kp ∼0.54 for NKN based random ceramics." @default.
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- W2167121036 date "2011-01-01" @default.
- W2167121036 modified "2023-10-18" @default.
- W2167121036 title "Sol–gel derived (Li, Ta, Sb) modified sodium potassium niobate ceramics: Processing and piezoelectric properties" @default.
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- W2167121036 doi "https://doi.org/10.1016/j.jallcom.2010.09.134" @default.
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