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- W2167162659 abstract "Coconut shell activated carbon (CSAC) granules were used as carriers to immobilize palladium complexes. Boehm titration showed that the hydroxyl content of the carbon surface reached 0.376 mmol g−1 after 20% HNO3 treatment. Ethylenediamine, benzyl malononitrile and propyl malononitrile were successfully grafted onto the oxidized CSAC. The bidentate nitrogen ligands complexed Pd2+ samples were characterized by FT-IR, XPS, ICP and N2 adsorption–desorption. In oxidative carbonylation of phenol, three bidentate ligand grafted catalysts were evaluated in a high pressure reaction vessel. The results showed that the ethylenediamine grafted catalyst had a phenol conversion of 12.06% and a diphenyl carbonate (DPC) selectivity of 91.03%. In comparison, the benzyl malononitrile grafted catalyst displayed a phenol conversion of 12.00% and a DPC selectivity of 90.65%. The propyl malononitrile grafted catalyst displayed a phenol conversion of 6.22% and a DPC selectivity of 81.02%. Additionally, the ethylenediamine and the benzyl malononitrile grafted catalysts were also investigated in a continuous packed-bed reactor. The results showed that the phenol conversion and the DPC selectivity were comparative to those obtained in a high pressure reaction vessel." @default.
- W2167162659 created "2016-06-24" @default.
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- W2167162659 date "2014-01-01" @default.
- W2167162659 modified "2023-10-14" @default.
- W2167162659 title "Preparation and application of coconut shell activated carbon immobilized palladium complexes" @default.
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- W2167162659 doi "https://doi.org/10.1039/c3cy00460k" @default.
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