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• W2167245248 abstract "Abstract The syntheses and some typical reactions of diastereomeric rhenium complexes [CpRe(NO)(CO){P(Ph)(R)(R′)}]BF 4 (R = Me, Ph; R′ = 2‐C 6 H 4 OMe, CH 2 C 4 H 3 S, CH 2 C 4 H 7 O) ( 3a − e ) are described. Reduction of the carbonyl ligand with NaBH 4 in THF gave the corresponding methyl complexes [CpRe(NO){P(Ph)(R)(R′)}(CH 3 )] ( 4a − e ). Acid treatment of the methyl complexes leads to liberation of methane and coordination of the additional donor site of the potentially bidentate phosphane ligand. Of the chelate complexes 5a − e , those with R′ = 2‐C 6 H 4 OMe ( 5a , d ) decomposed in solution at room temperature. In donor solvents, the chelate ring opens giving the stable solvated complexes [CpRe(NO){P(Ph)(R)(R′)}](solvent)]BF 4 (solvent = CH 3 CN, THF) ( 6b − e , 7d ). The new compounds are thus suitable starting materials for the syntheses of diastereomeric rhenium complexes [CpRe(NO){P(Ph)(R)(R′)}(L)]BF 4 . (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)" @default.
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• W2167245248 date "2004-12-01" @default.
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• W2167245248 title "Diastereomeric Halfsandwich Rhenium Complexes Containing Hemilabile Phosphane Ligands" @default.
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• W2167245248 doi "https://doi.org/10.1002/ejic.200400552" @default.
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