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• W2168180825 startingPage "145605" @default.
• W2168180825 abstract "We report on the synthesis of phase-pure TiO2 nanoparticles in anatase, rutile and brookite structures, using amorphous titania as a common starting material. Phase formation was achieved by hydrothermal treatment at elevated temperatures with the appropriate reactants. Anatase nanoparticles were obtained using acetic acid, while phase-pure rutile and brookite nanoparticles were obtained with hydrochloric acid at a different concentration. The nanomaterials were characterized using x-ray diffraction, UV–visible reflectance spectroscopy, dynamic light scattering, and transmission electron microscopy. We propose that anatase formation is dominated by surface energy effects, and that rutile and brookite formation follows a dissolution–precipitation mechanism, where chains of sixfold-coordinated titanium complexes arrange into different crystal structures depending on the reactant chemistry. The particle growth kinetics under hydrothermal conditions are determined by coarsening and aggregation–recrystallization processes, allowing control over the average nanoparticle size." @default.
• W2168180825 created "2016-06-24" @default.
• W2168180825 creator A5021873488 @default.
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• W2168180825 date "2008-03-05" @default.
• W2168180825 modified "2023-10-17" @default.
• W2168180825 title "Phase-pure TiO₂nanoparticles: anatase, brookite and rutile" @default.
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• W2168180825 doi "https://doi.org/10.1088/0957-4484/19/14/145605" @default.
• W2168180825 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/21817764" @default.
• W2168180825 hasPublicationYear "2008" @default.
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