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- W2168184006 abstract "Chemical Peptide Bond Formation with α-Trifluoromethyl Substituted α-Amino Acids The reaction of α-trifluoromethyl substituted N-tbutoxycarbonyl amino acids (Boc-TFM-Xaa-OH) 1 with dicyclohexylcarbodiimide results in formation of 2-tbutoxy-4-trifluoromethyl-5(4H)-oxazolones 2 within minutes. Compounds 2 react with amino acid esters to give Boc protected dipeptide esters 4. However, at room temperature compounds 2 decompose to give Leuchs anhydrides 3, via retro ene reaction. Therefore, α-trifluoromethyl substituted N-tbutoxycarbonyl amino acids (Boc-TFM-Xaa-OH) are of limited value for peptide synthesis." @default.
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- W2168184006 date "1995-01-01" @default.
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- W2168184006 title "Untersuchungen zur Kn�pfung der Peptidbindung mit ?-trifluormethylsubstituierten ?-Aminos�uren" @default.
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- W2168184006 doi "https://doi.org/10.1002/prac.19953370183" @default.
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