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- W2168233669 abstract "Abstract The crystal structure of the complex of formula {|Nd(NCS)3 (HMPA)3‖ |Nd(NCS)3 (HMPA)4|} was determined by three-dimensional X-ray diffraction methods and refined anisotropically to a R=0.040. The compound crystallizes in the trigonal system, space group R3 (No 146), with a=19.947(3), b=19.947(3), c=20.106(3) A, α=β=90, γ=120°, V=6928(4) A3, M=1891.4, Z=3, Dc=1.360 g cm−3, λ(MoKα)=0.71073 A, μ=1.4 cm−1, F (000)=2922.01. There are two independent Nd3+ ions located in the three fold axis. One of them, located at the origin (000) is coordinated to nitrogen atoms of three symmetry related NCS− anions which are below the (x y) plane (negative z) and also to the oxygen atoms of three symmetry related HMPA groups above that plane. The coordination polyhedron is a slightly distorted octahedron. The other Nd3+ ion is located at (00,0.5025(1)). It is coordinated to the nitrogen atoms of three symmetry related NCS− anions above the (xy 1/2) plane and to oxygen atoms of three symmetry related HMPA groups belo..." @default.
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- W2168233669 date "1987-04-01" @default.
- W2168233669 modified "2023-09-27" @default.
- W2168233669 title "Hexamethylphosphoramide Compounds: II. The Structure of a Complex Containing Two Different Coordination Polyhedra for Two Independent Neodymium(III) Ions" @default.
- W2168233669 doi "https://doi.org/10.1080/03086648708079236" @default.
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