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- W2169249883 abstract "Abstract Two new methods for synthesizing nanostructured HfO 2 have been developed. The first method entails exposing HfTe 2 powders to air. This simple process resulted in the formation of nanometer scale crystallites of HfO 2 . The second method involved a two-step heating process by which macroscopic, freestanding nanosheets of HfO 2 were formed as a byproduct during the synthesis of HfTe 2 . These highly two-dimensional sheets had side lengths measuring up to several millimeters and were stable enough to be manipulated with tweezers and other instruments. The thickness of the sheets ranged from a few to a few hundred nanometers. The thinnest sheets appeared transparent when viewed in a scanning electron microscope. It was found that the presence of Mn enhanced the formation of HfO 2 by exposure to ambient conditions and was necessary for the formation of the large scale nanosheets. These results present new routes to create freestanding nanostructured hafnium dioxide. PACS: 81.07.-b, 61.46.Hk, 68.37.Hk." @default.
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- W2169249883 date "2011-04-05" @default.
- W2169249883 modified "2023-10-18" @default.
- W2169249883 title "Synthesis of freestanding HfO2 nanostructures" @default.
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- W2169249883 doi "https://doi.org/10.1186/1556-276x-6-294" @default.
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