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• W2169677898 abstract "Abstract Gaseous FCO + ions from the ionization of mixtures of nitrogen trifluoride and carbon monoxide execute selective and efficient CO‐functionalization of the C–H bonds of benzene and toluene and of the N–H bond of ammonia. The occurrence of these carbonylation reactions has been unambiguously ascertained by Fourier‐transform ion cyclotron resonance (FT‐ICR) spectrometry, and the details of the structure and the mechanism of formation of the precursor FCO + ions have been investigated. FT‐ICR experiments show that these ions, structurally assigned as F–C–O + by collisionally activated dissociation (CAD) spectrometry, arise from the reaction of CO .+ with NF 3 and of NF + 2 with CO. Combining the latter F + transfer with the independently observed fluoride‐ion abstraction by FCO + from NF 3 results in a catalytic cycle in which gaseous NF + 2 ions promote the conversion of carbon monoxide into carbonic difluoride, F 2 CO, with nitrogen trifluoride as the source of F." @default.
• W2169677898 created "2016-06-24" @default.
• W2169677898 creator A5054349490 @default.
• W2169677898 creator A5075690467 @default.
• W2169677898 creator A5081365075 @default.
• W2169677898 date "1996-05-01" @default.
• W2169677898 modified "2023-10-12" @default.
• W2169677898 title "Ionic Fluorination of Carbon Monoxide as a Route to Gasphase Carbonylation of Inert CH and NH Bonds" @default.
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• W2169677898 doi "https://doi.org/10.1002/chem.19960020507" @default.
• W2169677898 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/29178229" @default.
• W2169677898 hasPublicationYear "1996" @default.
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