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• W2169777772 abstract "The total synthesis of the pre-anthraquinones atrochrysone 1 and torosachrysone 2 in both enantiomeric forms is described. The synthesis relies on the regioselective Tebbe methylenation of a chiral diester followed by an intramolecular enol ether acylation with N-triflyl-4-(dimethylamino)pyridinium triflate. The resulting 3-methoxycyclohex-2-enone 9 is condensed with suitable orsellinic acid derivatives to yield after deprotection the optically active 3,4-dihydroanthracen-1(2H)-ones 1 and 2. This flexible approach can be used for the synthesis of 13C-labelled compounds and should provide access to a series of analogues." @default.
• W2169777772 created "2016-06-24" @default.
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• W2169777772 date "2000-01-01" @default.
• W2169777772 modified "2023-10-03" @default.
• W2169777772 title "Stereoselective total syntheses of atrochrysone, torosachrysone and related 3,4-dihydroanthracen-1(2H )-ones" @default.
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• W2169777772 doi "https://doi.org/10.1039/b003053h" @default.
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