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- W2170332179 endingPage "135" @default.
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- W2170332179 abstract "Mono-polyhedral oligomeric sillsesquioxane-end capped poly(ε-caprolactone) (mPPCL) can form inclusion complexes (ICs) with α- and γ-cyclodextrins (CDs) but not with β-CD. These CD ICs have been characterized with X-ray diffraction, solid-state 13C cross-polarization/magic-angle-spinning NMR spectroscopy, 1H NMR spectroscopy, Fourier transform infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, and scanning electron microscopy. The poly(ε-caprolactone) (PCL) chain of mPPCL is included within the channel provided by the CDs to form a columnar, crystalline structure. The PCL/CD ratios determined by 1H NMR spectroscopy for the ICs with α- or γ-CDs are higher than the stoichiometries because of the steric hindrance of the bulky polyhedral oligomeric silsesquioxane chain end and result in a fraction of the ε-caprolactone units free from complexation with the CDs. On the basis of these analyses, we propose some possible structures for these CD/mPPCL ICs. © 2006 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 125–135, 2007" @default.
- W2170332179 created "2016-06-24" @default.
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- W2170332179 date "2006-01-01" @default.
- W2170332179 modified "2023-09-23" @default.
- W2170332179 title "Supramolecular aggregations through the inclusion complexation of cyclodextrins and polymers with bulky end groups" @default.
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- W2170332179 doi "https://doi.org/10.1002/pola.21820" @default.
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