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• W2170621361 abstract "The bis[hydrotris(1,2,4-triazolyl)borate]metal complexes [M{HB(C2H2N3)3}2] with M = Fe (5), Co (6), Cu (7), Zn (8) are obtained from MX2 and K[HB(C2H2N3)3] (9). The complexes are characterized by IR, UV/Vis, and MS. Temperature-variable magnetic measurements show a Curie-Weiss behavior for the paramagnetic complexes 6 and 7 with a temperature-dependent magnetic moment for 6. The iron complex 5 exhibits a spin crossover from diamagnetic to paramagnetic, starting at around 270 K. Single-crystal X-ray structures of the solvates 7 · 4 CH3OH and 9 · 2 H2O have been determined. The structure of 7 · 4 CH3OH shows the Jahn-Teller distorted copper complex 7 surrounded by methanol molecules through hydrogen bonding to exocyclic nitrogen atoms of the tris(1,2,4-triazolyl)borate ligand. The crystal system for 7 · 4 CH3OH is monoclinic, space group P21/n. Compound 9 · 2 H2O is a one-dimensional coordination polymer with the potassium atom bridged by the water molecules and the tris(1,2,4-triazolyl)borate ligand and crystallizes in the orthorhombic space group Ccm21." @default.
• W2170621361 created "2016-06-24" @default.
• W2170621361 creator A5090644272 @default.
• W2170621361 date "1994-08-01" @default.
• W2170621361 modified "2023-10-16" @default.
• W2170621361 title "Binary [Hydrotris(1,2,4‐triazolyl)borate]metal Complexes [M{HB(C ₂ H ₂ N ₃ ) ₃ } ₂ ] with M = Fe, Co, Cu, Zn: Synthesis, Characterization, Magnetochemistry, and X‐ray Structure of [Cu{HB(C ₂ H ₂ N ₃ ) ₃ } ₂ ·4CH ₃" @default.
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• W2170621361 doi "https://doi.org/10.1002/cber.19941270809" @default.
• W2170621361 hasPublicationYear "1994" @default.
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