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• W2170717378 abstract "Abstract A compound formulated as (C 4 H 12 N 2 )[Ge 2 (pmida) 2 (OH) 2 ] ⋅ 4 H 2 O (where pmida 4− = N ‐(phosphonomethyl)iminodiacetate and C 4 H 12 N 2 2+ =piperazinedium cation), containing the anionic [Ge 2 (pmida) 2 (OH) 2 ] 2− complex, has been synthesised by the hydrothermal approach and its structure determined by single‐crystal X‐ray diffraction analysis. Several high‐resolution solid‐state magic‐angle spinning (MAS) NMR techniques, in particular two‐dimensional 1 H–X( 13 C, 31 P) heteronuclear correlation (HETCOR) and 1 H– 1 H homonuclear correlation (HOMCOR) experiments incorporating a frequency‐switched Lee–Goldburg (FS‐LG) decoupling scheme, have been employed for the first time in such a material. Using these tools in tandem affords an excellent general approach to study the structure of other inorganic–organic hybrids. We assigned the NMR resonances with the help of C ⋅⋅⋅ H and P ⋅⋅⋅ H internuclear distances obtained through systematic statistical analyses of the crystallographic data. The compound was further characterised by powder X‐ray diffraction techniques, IR and Raman spectroscopy, and by elemental and thermal analyses (thermogravimetric analysis and differential scanning calorimetry)." @default.
• W2170717378 created "2016-06-24" @default.
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• W2170717378 date "2005-12-19" @default.
• W2170717378 modified "2023-10-17" @default.
• W2170717378 title "X-ray Diffraction and Solid-State NMR Studies of a Germanium Binuclear Complex" @default.
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• W2170717378 doi "https://doi.org/10.1002/chem.200500281" @default.
• W2170717378 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/16189839" @default.
• W2170717378 hasPublicationYear "2005" @default.
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