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- W2170817195 abstract "In this paper, we report the synthesis of symmetric and asymmetric telechelic polyisobutylenes (PIBs). A PIB with a primary hydroxy head group and an allyl end group (HO–PIB–Allyl, Mn = 4300 g mol−1; Mw/Mn = 1.2) was synthesized by living carbocationic polymerization of isobutylene (IB) using propylene epoxide as an initiator and allyltrimethylsilane as a terminating agent. Thiol–ene click chemistry using 2-mercaptoethanol and 1,2-ethanedithiol yielded an asymmetric HO–PIB–SEt–OH (Mn = 4646 g mol−1; Mw/Mn = 1.18) and a symmetric HO–PIB–OH (Mn = 8594 g mol−1; Mw/Mn = 1.2) respectively. A symmetric allyl telechelic PIB (Mn = 8669 g mol−1; Mw/Mn = 1.2) was prepared by enzymatic transesterification of divinyl adipate with the primary hydroxy group of HO–PIB–Allyl." @default.
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- W2170817195 date "2014-05-27" @default.
- W2170817195 modified "2023-10-14" @default.
- W2170817195 title "Synthesis of functionalized polyisobutylenes using the propylene epoxide/TiCl<sub>4</sub>initiating system" @default.
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- W2170817195 doi "https://doi.org/10.1039/c4py00363b" @default.
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