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- W2171342942 abstract "Reaction of a trinuclear iron(II) complex, Fe3 Br3 L (1), with KC8 under N2 leads to dinitrogen activation products (2) from which Fe3 (NH)3 L (2-1; L is a cyclophane bridged by three β-diketiminate arms) was characterized by X-ray crystallography. (1) H NMR spectra of the protonolysis product of 2 synthesized under (14) N2 and (15) N2 confirm atmospheric N2 reduction, and ammonia is detected by the indophenol assay (yield ∼30 %). IR and Mössbauer spectroscopy, and elemental analysis on 2 and 2-1 as well as the tri(amido)triiron(II) 3 and tri(methoxo)triiron 4 congeners support our assignment of the reduction product as containing protonated N-atom bridges." @default.
- W2171342942 created "2016-06-24" @default.
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- W2171342942 date "2014-12-11" @default.
- W2171342942 modified "2023-10-16" @default.
- W2171342942 title "Dinitrogen Activation Upon Reduction of a Triiron(II) Complex" @default.
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- W2171342942 doi "https://doi.org/10.1002/anie.201409676" @default.
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