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- W2171493571 abstract "Woodward's Reagent K was used to activate the carboxyl group of protected amino acids. Subsequent reaction with trimethylsilylisothiocyanate consistently resulted in high yields of the 1-NFmoc-2-thiohydantoins. The protecting group(s) were readily removed with piperidine and TFA and the final thiohydantoin products were recovered in pure form after chromatography and crystallization. These especially mild conditions provide an improved synthetic route to the thiohydantoins, especially for the amino acids bearing sensitive side-chain groups." @default.
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- W2171493571 date "1990-01-01" @default.
- W2171493571 modified "2023-09-25" @default.
- W2171493571 title "Synthesis of the 2-thiohydantoins of amino acids using woodward's reagent K" @default.
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- W2171493571 doi "https://doi.org/10.1016/s0040-4039(00)97485-9" @default.
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