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- W2171882949 abstract "A convenient procedure has been developed for the synthesis of 14C-3-chloropropan-1, 2-diol (α-chlorohydrin, I) from 14C-glycerol which can also be applied to the preparation of 14C-3-bromopropan-1, 2-diol (α-bromohydrin, III). These two compounds can be converted, respectively, by nucleophylic displacement with sodium iodide 14C-3-iodopropan-1, 2-diol (α-iodohydrin, II) and by alkaline epoxidation to 14C-2, 3-epoxypropan-1-01 (glycidol, IV). The use of readily available u, 1, 3- or 2- 14C-glycerol thus enables the title compounds to be synthesised readily and any desired labelling pattern as useful 3-carbon intermediates for further radioactive syntheses." @default.
- W2171882949 created "2016-06-24" @default.
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- W2171882949 date "1973-10-01" @default.
- W2171882949 modified "2023-09-27" @default.
- W2171882949 title "The synthesis of14C -3- chloro -, 3 - bromo - and 3 - iodo -propan - 1, 2 - diol and 2, 3 - epoxypropan - 1 -01" @default.
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- W2171882949 doi "https://doi.org/10.1002/jlcr.2590090411" @default.
- W2171882949 hasPublicationYear "1973" @default.
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