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• W2172605609 startingPage "7962" @default.
• W2172605609 abstract "Abstract A general and modular synthesis of substituted benzene and pyridine 2′‐ C ‐methyl‐ C ‐ribonucleosides was developed. Benzyl‐protected haloaryl‐ C ‐nucleoside intermediates were prepared by the addition of bromo(het)aryllithium reagents to a protected lactone, followed by acetylation and reduction. These halogenated intermediates were further transformed by Pd‐catalysed cross‐couplings, aminations, or hydroxylations. The final deprotection was rather troublesome, and different procedures involving catalytic hydrogenation on Pd/C, or treatment with BCl 3 , were optimized for each derivative. The final C ‐nucleosides were also all converted into the corresponding NTPs. None of the C ‐nucleosides showed any activity in the HCV replicon assay, and none of the NTPs showed any significant inhibition of the HCV polymerase." @default.
• W2172605609 created "2016-06-24" @default.
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• W2172605609 date "2015-11-17" @default.
• W2172605609 modified "2023-10-12" @default.
• W2172605609 title "Synthesis of Benzene and Pyridine 2′-<i>C</i>-Methyl-<i>C</i>-ribonucleosides and -nucleotides" @default.
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• W2172605609 doi "https://doi.org/10.1002/ejoc.201501219" @default.
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