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- W217291281 abstract "The new series of argyrodite compounds with the formula Ag7−ξ MX6−ξ Iξ (M = Ta, Nb; X = S, Se) have been prepared by a sealed silica tube method at 500–550 °C for 4 days. The compounds Ag7NbS6, Ag6.5TaSe5.5I0.5 and Ag7TaSe6 crystallize in the cubic system with the unit-cell dimensions of a = 10.5001 ± 0.0006 Å, a = 10.8422 ± 0.0009 Å and a = 10.8277 ± 0.0005 Å, respectively. The observed densities are 5.90 g cm−3 for Ag7NbS6, 7.02 g cm−3 for Ag6.5TaSe5.5I0.5 and 7.33 g cm−3 for Ag7TaSe6. The unit cell contains four formula units. The X-ray diffraction patterns of the former two compounds are very similar to that of Ag7TaS6 (space group F43m). Refinement was performed using X-ray powder diffraction data, the positional parameters for Ag7NbS6 being determined. These compounds are mixed conductors. The ionic conductivity σAg+ and transport number were measured at temperatures from room temperature to 220°C." @default.
- W217291281 created "2016-06-24" @default.
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- W217291281 date "1992-02-01" @default.
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- W217291281 title "Crystal structures and silver ionic conductivities of the new compounds Ag7NbS6, Ag7TaSe6 and Ag7−ξTaSe6−ξIξ (0.1 ⩽ ξ ⩽ 0.5)" @default.
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- W217291281 doi "https://doi.org/10.1016/0925-8388(92)90273-c" @default.
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