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• W2174715268 startingPage "896" @default.
• W2174715268 abstract "Nanocrystalline powders of Ba 1− x Mg x Zr 0.1 Ti 0.9 O 3 ( x = 0.025–0.1) were synthesized via citrate assisted sol–gel method. Interestingly, the one with x = 0.05 in the system Ba 1− x Mg x Zr 0.1 Ti 0.9 O 3 exhibited fairly good piezoelectric response aside from the other physical properties. The phase and structural confirmation of synthesized powder was established by X‐ray powder diffraction ( XRD ) and Raman Spectroscopic techniques. Two distinct Raman bands i.e., 303 and 723 cm −1 characteristic of tetragonal phase were observed. Thermogravimetric analysis ( TGA ) was performed to evaluate the phase decomposition of the as‐synthesized Ba 0.95 Mg 0.05 Zr 0.1 Ti 0.9 O 3 sample as a function of temperature. The average crystallite size associated with Ba 0.95 Mg 0.05 Zr 0.1 Ti 0.9 O 3 was calculated using Scherrer formula based on the XRD data and was found to be 25 nm. However, Scanning and Transmission Electron Microscopy studies revealed the average crystallite size to be in the range of 30–40 nm, respectively. Kubelka–Munk function was employed to determine the optical band gap of these nanocrystallites. A piezoelectric response of 26 pm/V was observed for Ba 0.95 Mg 0.05 Zr 0.1 Ti 0.9 O 3 nanocrystal by Piezoresponse Force Microscopy ( PFM ) technique. Photoluminescence ( PL ) study carried out on these nanocrystals exhibited a blue emission (470 nm) at room temperature." @default.
• W2174715268 created "2016-06-24" @default.
• W2174715268 creator A5000812892 @default.
• W2174715268 creator A5015162781 @default.
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• W2174715268 date "2015-11-18" @default.
• W2174715268 modified "2023-10-01" @default.
• W2174715268 title "Structural, Optical, and Piezoelectric Response of Lead‐Free Ba _0.95 Mg _0.05 Zr _0.1 Ti _0.9 O ₃ Nanocrystalline Powder" @default.
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• W2174715268 doi "https://doi.org/10.1111/jace.14018" @default.
• W2174715268 hasPublicationYear "2015" @default.
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