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- W2175964598 abstract "[63059-25-6], [62973-69-7] C6H5IO3S (MW 284.0716)InChI = 1S/C6H5IO3S/c7-5-3-1-2-4-6(5)11(8,9)10/h1-4H,(H,8,9,10)InChIKey = ZJTNYBYLBTVLRD-UHFFFAOYSA-N(synthetic precursor of λ3-iodanes for oxidative coupling reagents1-4 and λ5-iodanes for alcohol,5 sulfide,6 and secondary amine6 oxidation reagents; precatalyst of 2-iodoxybenzenesulfonic acid (IBS)7 for catalytic alcohol oxidations8-10)Alternate Name: o-iodobenzenesulfonic acid.Physical Data: white solid; mp 344–345 °C.11Solubility: sol in DMSO, MeOH, EtOH, CH3CN, CH3NO2, H2O; less soluble in CHCl3, EtOAc, Et2O.Form Supplied in: dihydrate.Handling, Storage, and Precautions: store in a dark place.Preparative Methods: the sodium or potassium salt of 2-iodobenzenesulfonic acid can be obtained from 2-aminobenzenesulfonic acid by the Sandmeyer reaction (eq 1).8, 11 2-Iodobenzenesulfonic acid can be obtained via protonation with conc HCl1 or anion-exchange resin (eq 1).8 Arene-substituted 2-iodobenzenesulfonic acid derivatives can also be prepared in a similar manner.1, 8(1)" @default.
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- W2175964598 date "2012-09-14" @default.
- W2175964598 modified "2023-09-23" @default.
- W2175964598 title "2-Iodobenzenesulfonic Acid" @default.
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