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• W2176583695 abstract "A cytotoxic marine alkaloid (−)-lepadiformine A (1) possesses a unique structure characterized by the trans-1-azadecalin AB ring system fused with the AC spiro-cyclic ring. In this research, we found that a cycloisomerization reaction from amino ynone 2 to a 1-azaspiro[4.5]decane skeleton 3, corresponding to the AC ring system of 1, is promoted by Hg(OTf)2. Thus, we have accomplished the efficient total synthesis of (−)-lepadiformine A in 28% overall yield by featuring the novel Hg(OTf)2-catalyzed cycloisomerization." @default.
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• W2176583695 date "2015-11-19" @default.
• W2176583695 modified "2023-09-30" @default.
• W2176583695 title "Total Synthesis of (−)-Lepadiformine A Utilizing Hg(OTf)₂-Catalyzed Cycloisomerization Reaction" @default.
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• W2176583695 doi "https://doi.org/10.1021/acs.orglett.5b02867" @default.
• W2176583695 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/26584002" @default.
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