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• W2176693285 abstract "This article compares the use of batch-injection analysis (BIA) with a conventional batch system for the anodic stripping voltammetric (ASV) determination of Pb, Cu and Hg in biodiesel using screen-printed gold electrode (SPGE). The optimized BIA conditions were 200 µL of injection volume of the digested samples at 5 µL s−1 directly on the working electrode of the SPGE immersed in 0.1 mol L−1 HCl solution. Therefore, BIA-ASV presented the advantages of low sample consumption, which extended the SPGE lifetime to a whole working day of analyses, and potential for on-site analysis using battery-powered micropipettes and potentiostats. Although presenting lower sensitivity than conventional systems, the BIA-ASV presented detection limit values of 1.0, 0.5 and 0.7 µg L−1, respectively for Pb, Cu and Hg, a linear range between 20 and 280 µg L−1, and adequate recovery values (90–110 %) for spiked biodiesel samples." @default.
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• W2176693285 date "2015-11-26" @default.
• W2176693285 modified "2023-10-18" @default.
• W2176693285 title "Voltammetric Determination of Pb, Cu and Hg in Biodiesel Using Gold Screen-printed Electrode: Comparison of Batch-injection Analysis with Conventional Electrochemical Systems" @default.
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• W2176693285 doi "https://doi.org/10.1002/elan.201501012" @default.
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