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• W2177093846 abstract "We completed the first total synthesis of puerarin (1), an isoflavone C-glycoside. The key intermediate, β-d-glucopyranosyl-2,6-dimethoxybenzene (9), was obtained by coupling of a lithiated aromatic reagent (3) with pyranolactone (2) in 56% yield. Condensation of (16) with p-methoxybenzaldehyde gave the chalcone (17). The protected chalcone (18) was cyclized to (19) in the presence of Tl(NO3)3. Demethylation of (19) was accomplished by refluxing with TMSI in CH3CN to give puerarin (1)." @default.
• W2177093846 created "2016-06-24" @default.
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• W2177093846 date "2003-09-01" @default.
• W2177093846 modified "2023-09-26" @default.
• W2177093846 title "Total synthesis of puerarin, an isoflavone C-glycoside" @default.
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• W2177093846 doi "https://doi.org/10.1016/s0040-4039(03)01715-5" @default.
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