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- W2178700057 abstract "A tri-functional ligand (Ph2PCH2)NH(2-C5H4N), DPAP-2, has been synthesized via the Mannich condensation reaction and its coordination behavior has been studied with various Ag(I) salts. The ligand is capable of P-coordination, P,N-chelation, and P,N-bridging to form Ag(I) complexes that range from discrete to 1-dimensional polymeric structures. In the 1:2 reaction of AgBF4 with DPAP-2, a 4-coordinate Ag(I) structure with P,N′-chelation is isolated (1). A counterion effect is observed in the equimolar reactions of AgX (2: X = BF4− and 3: X = tfa−) with DPAP-2, where the structures isolated are a dimer and a 1-dimensional polymer, respectively. When an equivalent of 5,5′-dimethyl-2,2′-dipyridyl (5,5′-dmbpy) was incorporated to the equimolar reaction of AgX and DPAP-2, three isostructural complexes resulted (4: X = BF4−, and supplementary structures S1: X = tfa−, and S2: X = OTf−). In the 2:1:2 reaction of AgX (5: X = BF4− and 6: X = tfa−) with DPAP-2 and 5,5′-dmbpy, two distinct complexes are isolated where DPAP-2 adopts a syn- and anti-arrangement, respectively." @default.
- W2178700057 created "2016-06-24" @default.
- W2178700057 creator A5033537903 @default.
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- W2178700057 date "2015-12-01" @default.
- W2178700057 modified "2023-10-02" @default.
- W2178700057 title "Silver coordination complexes of 2-(diphenylphosphinomethyl)aminopyridine with weakly interacting counterions" @default.
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- W2178700057 doi "https://doi.org/10.1016/j.poly.2015.09.048" @default.
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