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- W2181446957 abstract "Irreversible crystal-to-crystal transformations of 3D lead(II) coordination polymers with the ligand 1H-1,2,4-triazole-3- carboxylic acid (HL), from (Pb(L)(µ 2-Cl)(H2O)) n (1) to (Pb(L)(µ2- Br)(H2O)) n (2) and (Pb(L)(µ1,1-NCS)(H2O)) n (3) by solid-state anion-replacement processes under mechanochemical reactions, have been studied. These irreversible solid-state structural transformations of compound 1 to compounds 2 and 3, have been verified by PXRD measurements. PbCl 2, PbBr 2 and PbS nanoparticles were obtained by thermal decomposition of compounds 1, 2 and 3 in oleic acid as surfactant at 200 °C under air atmosphere, respectively. These nanoparticles were characterized by powder X-ray diffraction (PXRD) and scanning electron microscopy (SEM)." @default.
- W2181446957 created "2016-06-24" @default.
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- W2181446957 date "2013-01-01" @default.
- W2181446957 modified "2023-09-27" @default.
- W2181446957 title "Mechanochemical Solid-State Transformations of 3D Lead(II) Triazole Carboxylate Coordination Polymers; Precursors for the Preparation of Lead(II) Chloride/Bromide/ Sulfide Nanostructure" @default.
- W2181446957 hasPublicationYear "2013" @default.
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