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• W2181629328 abstract "Article history: Received 8 December 2014 Accepted 11 December 2014 Available online 12 December 2014 The microwave synthesis route employed for the preparation of cadmium metal oxide nanoparticles. Crystalline CdCO3 has been synthesized at nanoscale through a reaction of cadmium acetate with tetramethyammoniumhydroxide (TMAH) and surfactant polyvinyl alcohol (PVA) at different temperatures and with different aging times. By heating synthesized CdCO3 at different temperatures 400 °C and 700 °C, the CdO nanocrystals are obtained. Debye-Scherrer’s formula is used to calculate the particle size and the calculated value is 22.87nm. Band gap energy has been calculated for the prepared CdCO3 and CdO from the UV-Visible spectrum. The band gap value for CdO obtained as 0.0766 eV. While CdO converted into nano-sized particles, the free movements of asymmetric and symmetric stretching are blocked which behavior is observed from FT-IR spectrum. TEM images give the clear morphological appearance of CdO nanoparticles. The present successive simple process can be easily implement to prepare CdO nanoparticles with the low cost of investment in a short time period." @default.
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• W2181629328 date "2015-01-01" @default.
• W2181629328 modified "2023-09-23" @default.
• W2181629328 title "Microwave Mediated Synthesis and Characterizations of CdO Nanoparticles" @default.
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