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- W2182606034 abstract "An isocratic reverse phase liquid chromatography (RP-LC) method has been developed and subsequently validated for the determination of Lacosamide in Bulk and its pharmaceutical formulation. Separation was achieved with a Develosil ODS HG-5 ((Make: Nomura chemicals (Japan); 150 mmx4.6 mm I.D; particle size 5 µm)) Column and Sodium di-hydrogen phosphate monohydrate buffer (pH adjusted to 3.0 with diluted orthophosphoric acid): Acetonitrile (700:300) v/v as eluent at flow rate 1.0 mL/min and the Column temperature was 40°C. UV detection was performed at 210nm and sample temperature was maintained at 5°C . The method is simple, rapid, and selective. The described method of Lacosamide is linear over a range of 3.996 µg/mL to 47.952 µg/mL . The method precision for the determination of assay was below 2.0%RSD. The percentage recoveries of active pharmaceutical ingredient (API) from dosage forms ranged from 100.0 to 101.3%. The method is useful in the quality control of Bulk and pharmaceutical formulations." @default.
- W2182606034 created "2016-06-24" @default.
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- W2182606034 date "2011-01-01" @default.
- W2182606034 modified "2023-09-24" @default.
- W2182606034 title "DEVELOPMENT AND VALIDATION OF RP-HPLC METHOD FOR ESTIMATION OF LACOSAMIDE IN BULK AND ITS PHARMACEUTICAL FORMULATION" @default.
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