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- W2185674772 abstract "A Total Reflection X-ray Fluorescence (TXRF) method, for the determination of chlorine in (U,Pu)C has been developed. The method involves calibration of the instrument with standard solutions and validation of TXRF determination of chlorine, using synthetic standard solutions. Cl K a line excited with W L a source was used, for TXRF determinations of chlorine. Chlorine present in trace amounts in (U,Pu)C samples was first separated by pyrohydrolysis. The evolved chlorine, in the form of HCl, was collected in 5 μM NaOH solution. This solution was analyzed for chlorine by Total Reflection X-ray Fluorescence Spectrometry, using cobalt as an internal standard. The TXRF detection limit of chlorine was found to be 3.6 pg with sample size of 30 μL. In order to assess the applicability of TXRF method for chlorine determinations in other nuclear materials, one U 3 O 8 trace element standard was also analyzed for chlorine, in a similar way. The precision of the method was found to be 25% (1s) at ng level in most of the cases." @default.
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- W2185674772 date "2007-01-01" @default.
- W2185674772 modified "2023-09-26" @default.
- W2185674772 title "CHLORINE DETERMINATION IN (U,PU)C FUEL BY TOTAL REFLECTION X-RAY FLUORESCENCE" @default.
- W2185674772 hasPublicationYear "2007" @default.
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