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• W2186089503 abstract "In this study, nanosized powders β -Tricalcium phosphate β -Ca3(PO4)2 (β -TCP) were synthesized via aqueous precipitation technique using a diammonium phosphate solution (NH4)2HPO4 and a calcium nitrate tetrahydrate solution Ca(NO3)2,4H2O as precursor materials, with a Ca/P molar ratio 1.50 from the initial reagents. The effects of various aging time on the nanocrystalline β -TCP properties was studied during synthesis process. 2, 24, 48, and 72 h aging times were chosen. The crystallinity, composition phases, morphology and particle size of the products were characterized by X-ray diffraction (XRD), transmission electron microscope (TEM), Fourier transform infrared spectroscopy (FT-IR), differential thermogravimetry, thermal analysis (TG-DTA) and inductively coupled plasma ICP AES atomic emission spectroscopy. The influence of various aging time on the Ca/P ratio and composition of TCP phase was also been investigated." @default.
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• W2186089503 date "2014-01-01" @default.
• W2186089503 modified "2023-09-26" @default.
• W2186089503 title "Synthesis and characterization of nano-sized β-Tricalcium phosphate: Effects of the aging time" @default.
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