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- W2186163376 abstract "Development and validation of a multi-residues analytical method for ten pesticides in aniseeds according to European guidelines was achieved. Baseline separation was achieved for most of the tested pesticides. GC/ECD equipped with 2 different polarity columns was used in this study for quantification and confirmation of the results. Method showed good linearity down to 0.025 µgml −1 and up to 0.25 µgml −1 levels. 2 g sample size offered extra ease of the method performance and minimized interferences and matrix load to the chromatograph injector and columns. The chosen pesticides possess wide range of physico-chemical properties in order to demonstrate the validity of the method to be applied for a wider range of pesticides. Matrix matched external standard method was employed for quantification using pesticide free blank extract. Accuracy (recovery) data ranged from 82.29 % (chlorothalonil) to 116.3 % (cypermethrin). Also, the method showed acceptable repeatability not higher than 13.94 % (deltamethrin). The overall mean recovery (102.54%) and its RSD (8.41%) show the adequacy of the whole method with expanded uncertainty of 16.82 %. The presented method showed acceptable accuracy results that fall in the required range between 80 % and 120 % and precision (RSD) not higher than 20 %. The obtained results meet the EU standard requirements and legislations to consider a method accurate and reproducible." @default.
- W2186163376 created "2016-06-24" @default.
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- W2186163376 date "2014-01-01" @default.
- W2186163376 modified "2023-09-27" @default.
- W2186163376 title "Determination of Multiclass Pesticides in Dry Herbs Using GC-ECD" @default.
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- W2186163376 hasPublicationYear "2014" @default.
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