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- W2186199979 abstract "Indole-tetrahydroisoquinoline derivatives based on homoveratrilamine and 3-indolylacetic acid by the Bischler-Napieralski reaction have been obtained and their structures were confirmed by IR and NMR spectra. A mixture of homoveratrylamine (1, 3.04 g, 0.016 mol) and 2-(1H-indol-3-yl)acetic acid (3 g, 0.017 mol) in MeOH (5 mL) underwent spontaneous heating. The mixture was heated on an oil bath for 3 h at 178 °C. The course of the reaction was monitored by TLC. Then treated with CHCl3 (100 mL), and washed with HC1 solution (3%), NaOH solution (2%), and H20 until neutral. The CHC13 was evaporated. The residue was crystallized from Me2CO or hexane. The resulting crystals were filtered off. The yield of 3 is 70% (4 g), mp 116-119 °C (Me2CO), Rf 0.65 (system 1)." @default.
- W2186199979 created "2016-06-24" @default.
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- W2186199979 date "2014-01-01" @default.
- W2186199979 modified "2023-09-27" @default.
- W2186199979 title "Synthesis of Tetrahydroisoquinolines Based on Homoveratrilamine and 3-Indolylacetic Acid" @default.
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