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• W2186290413 endingPage "863" @default.
• W2186290413 startingPage "858" @default.
• W2186290413 abstract "We report herein a practical method for taming Langlois' reagent CF3 SO2 Na to generate CuSCF3 by a triphenylphospine-mediated deoxygenative reduction process. This chemistry highlights a novel utilization of the inherent CF3 S skeleton of Langlois' reagent as a CF3 S feedstock under mild conditions. The CuSCF3 intermediate generated by this protocol can react with a wide array of supporting ligands to furnish several air-stable [LCu(SCF3 )] complexes as valuable trifluoromethylthiolating agents. In addition, the CuSCF3 intermediate can be directly employed for the trifluoromethylthiolation of (hetero)aryl iodides with operational simplicity and atomic efficiency." @default.
• W2186290413 created "2016-06-24" @default.
• W2186290413 creator A5011156551 @default.
• W2186290413 creator A5056867614 @default.
• W2186290413 creator A5058505086 @default.
• W2186290413 creator A5070478005 @default.
• W2186290413 creator A5075913121 @default.
• W2186290413 creator A5084146813 @default.
• W2186290413 date "2015-12-21" @default.
• W2186290413 modified "2023-10-07" @default.
• W2186290413 title "Triphenylphosphine-Mediated Deoxygenative Reduction of CF₃ SO₂ Na and Its Application for Trifluoromethylthiolation of Aryl Iodides" @default.
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• W2186290413 doi "https://doi.org/10.1002/chem.201504790" @default.

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