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- W2186487982 abstract "A high performance liquid chromatographic (HPLC) me thod for the analysis of Lansoprazole and its assoc iated impurities was examined with the aim of economic an alysis, while maintaining good efficiency. The sepa ration was carried out using a Chromatopak Peerless -C18 analy tical column with a mobile phase composed of aceton itrile: buffer (500:500v/v) (buffer pH 10.0, adjusted with orthophosphoric acid) and was isocratically eluted at a flow rate of 1.0 mL min -1 . Column oven temperature was 30oC. A small sample volume of 20 µL was used for each sample run, being injected into the HPLC system. The chrom atogram was monitored with UV detection at a wavele ngth of 254 nm and the total run time was 30 min. The meth od was validated according to ICH (international co nference on harmonization) guidelines with respect to precis ion, accuracy, linearity, specificity, robustness a nd limits of detection and quantification. All parameters examin ed were found to be well within the stated guidelin es." @default.
- W2186487982 created "2016-06-24" @default.
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- W2186487982 date "2013-01-01" @default.
- W2186487982 modified "2023-09-23" @default.
- W2186487982 title "Development and validation of a rapid liquid chromatographic method for the analysis of Lansoprazole and its related production impurities" @default.
- W2186487982 hasPublicationYear "2013" @default.
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