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- W2187002661 abstract "6 2, 6 3, 7 5 8 6 8 and 7 9 have 13 C NMR). RAFT Polymerization. The following procedure is typical. Aliquots (0.5 mL) of stock solution from the control experiment (MMA (7.5 mL, 7.01 M), AIBN (11 mg, 0.0066 M), cyanoisopropyl methyl trithiocarbonate (6) (0.023 g, 0.01M) in benzene (2.5 mL)) were transferred to ampoules containing scandium triflate (0.05g, to give 0.21 M), degassed with three freeze-evacuate-thaw cycles and sealed. The ampoules were heated at 60±1 °C in a thermostatted oil bath. End Group Reduction. The following procedure is typical. A mixture of the PMMA synthesized with 7 (Mn 3400, Mw/Mn 1.18, 170 mg), N- ethylpiperidine hypophosphite (45 mg) and ACHN (4 mg) in toluene (1 mL) was degassed and heated at 100 0 C for 2 hrs. The solution was extracted with water and the toluene removed to give a colorless polymer Mn 3380, Mw/Mn 1.16." @default.
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- W2187002661 date "2008-09-22" @default.
- W2187002661 modified "2023-09-27" @default.
- W2187002661 title "ADVANCES IN RAFT POLYMERIZATION: IMPROVED NANOSTRUCURED MATERIALS." @default.
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