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- W2188432270 abstract "The replacement of cations at the B-sites in the spinel ferrite ZnFe2O4 by Mn3+ ions brings in several interesting changes, the most striking among them being a transformation from the spinel cubic structure to a body-centered tetragonal one. Concomitantly, there are variations in the nanocrystallite sizes and also in the lattice parameters. These are examined through high-precision X-ray diffraction measurements and transmission electron microscopic analysis. A more interesting aspect is the success of positron annihilation spectroscopy comprising of the measurements of positron lifetime and coincidence Doppler broadening measurements in understanding the effects of cation replacement and the resultant generation of vacancy-type defects. There are definite changes in the positron lifetimes and intensities which show positron trapping in trivacancy-type defect clusters and the nanocrystallite surfaces. The presence of ortho-positronium atoms within the extended intercrystallite region is also identified, ..." @default.
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- W2188432270 date "2015-11-24" @default.
- W2188432270 modified "2023-09-24" @default.
- W2188432270 title "Positron annihilation spectroscopic studies of Mn substitution-induced cubic to tetragonal transformation in ZnFe2–xMnxO4(x = 0.0–2.0) spinel nanocrystallites" @default.
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- W2188432270 doi "https://doi.org/10.1080/14786435.2015.1110631" @default.
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