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• W2191330795 abstract "The reactivity of the mer-[RuCl3(dppb)H2O] complex (1) with di-hydrogen shows that the products formed depend on the conditions of the reaction, i.e., solvents and presence or absence of a base. The new mixed-valence complexes [(diop)ClRu–(μ-Cl)3–RuCl(dppb)] (3), [(binap)ClRu–(μ-Cl)3–RuCl(dppb)] (4), [(PPh3)2ClRu–(μ-Cl)3–RuCl(dppb)] (6), [(dppn)ClRu–(μ-Cl)3–RuCl(dppb)] (7), [(P-ptol3)2ClRu–(μ-Cl)3–RuCl(dppb)] (8), [(SbPh3)2ClRu–(μ-Cl)3–RuCl(dppb)] (9), [(η6-C6H6)Ru–(μ-Cl)3–RuCl(dppb)] (11) and the known mixed-valence [(dppb)ClRu–(μ-Cl)3–RuCl(dppb)] (5) and [(diop)ClRu–(μ-Cl)3–RuCl(diop)] (10) were synthesized from complexes (1) or (2) using a methodology developed in our research group. The known complexes [(dppb)ClRu–(μ-Cl)2–RuCl(dppb)] (12), [(dppb)(CO)Ru–(μ-Cl)3–RuCl(dppb)] (13) and [H2NEt2][(dppb)ClRu–(μ-Cl)3–RuCl(dppb)] (14) were synthesized by changing the reaction conditions between mer-[RuCl3(dppb)H2O] (1) and di-hydrogen. The crystal structures of (5) and (11) were determined by single-crystal X-ray diffraction. Some of the complexes described here are effective pre-catalysts for the hydrogenation of imines. Preliminary results on the homogeneous hydrogenation of the imines Ph–CH2–NCH–Ph and Ph–NCH–Ph are presented." @default.
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• W2191330795 date "2004-12-01" @default.
• W2191330795 modified "2023-10-17" @default.
• W2191330795 title "mer-[RuCl3(P–P)H2O] (P–P=dppb or diop) as a starting material for the synthesis of binuclear complexes. Crystallographic structures of [(dppb)ClRu–μ(Cl)3–RuCl(dppb)] and [(η6-C6H6)Ru–μ(Cl)3–RuCl(dppb)]." @default.
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• W2191330795 doi "https://doi.org/10.1016/j.poly.2004.09.028" @default.
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