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W2192285963 abstract "The reaction of lanthanocenes Cp3Ln (Cp  C5H5, Ln  Dy, Yb) with the equimolar alcohols HOR [R  CH2CH2CH2CH2CH3,, CH2CH2CH(Me)2] in THF forms three new dinuclear organolanthanide alkoxides, namely [Cp2Yb(μ-OCH2CH2CH2CH2CH3)]2 (I) and [Cp2Ln(μ-OCH2CH2CH(Me)2)]2 [Ln  Dy (II), Yb (III)]. These three new complexes have been characterized by elemental analysis, IR and MS spectra, indicating they are oxygen-bridging dimers. Complexes I and II have also been studied by X-ray crystallography. The ytterbium atom is coordinated by two Cp rings and two oxygen atoms of bridging alkoxide groups to form a distorted pseudo tetrahedral geometry. The average YbC(Cp) distances in I and III are 2.59(2) and 2.60(2) Å, respectively. The average YbO distances for I and III are 2.18(1) and 2.197(6) Å, respectively." @default.
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W2192285963 date "1996-01-01" @default.
W2192285963 modified "2023-10-02" @default.
W2192285963 title "Synthesis and characterization of dinuclear organolanthanide alkoxides, X-ray crystal structures of [(C5H5)2Yb(μ-OCH2CH2CH2CH2CH3)]2 and [(C5H5)Yb(μ-OCH2CH2CH(Me)2]2" @default.
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W2192285963 doi "https://doi.org/10.1016/0277-5387(95)00241-j" @default.
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