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- W2196201913 abstract "Conditions were investigated for the electrochemical reduction of uranium(VI) to uranium(IV) in sodium carbonatebicarbonate solutions at mercury and platinum cathodes in a cell with cation exchange membranes separating cathode and anode compartments. A current density plateau was found only for the mercury cathode, in the potential range between --1.20 and --1.85 v vs SCE, which permits specific reduction of uranium(VI) with current efficiencies of over 80%. The reduction was performed so that no precipitation occurred in the electrolysis cell itself, the precipitation of uranium dioxide being carried out in a separate vessel. The possibilities of a large-scale process used based on the experimental work are discussed. (Uran. Abstr., 3: No. 2, Jan. 1964)" @default.
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- W2196201913 date "1963-09-01" @default.
- W2196201913 modified "2023-10-17" @default.
- W2196201913 title "PREPARATION OF URANIUM DIOXIDE BY ELECTROCHEMICAL REDUCTION OF URANIUM(VI) TO URANIUM(IV) IN CARBONATE SOLUTIONS AND SUBSEQUENT PRECIPITATION. I. THE ELECTROLYSIS OF URANIUM(VI) IN SODIUM CARBONATE SOLUTIONS" @default.
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