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• W2196237611 endingPage "22363" @default.
• W2196237611 startingPage "22351" @default.
• W2196237611 abstract "The synthesis and reactivity of tetrazol-5-yl-phosphorus ylides towards N-halosuccinimide/TMSN₃ reagent systems was explored, opening the way to new haloazidoalkenes bearing a tetrazol-5-yl substituent. These compounds were obtained as single isomers, except in one case. X-ray crystal structures were determined for three derivatives, establishing that the non-classical Wittig reaction leads to the selective synthesis of haloazidoalkenes with (Z)-configuration. The thermolysis of the haloazidoalkenes afforded new 2-halo-2-(tetrazol-5-yl)-2H-azirines in high yields. Thus, the reported synthetic methodologies gave access to important building blocks in organic synthesis, vinyl tetrazoles and 2-halo-2-(tetrazol-5-yl)-2H-azirine derivatives." @default.
• W2196237611 created "2016-06-24" @default.
• W2196237611 creator A5015747915 @default.
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• W2196237611 date "2015-12-12" @default.
• W2196237611 modified "2023-10-15" @default.
• W2196237611 title "Synthesis of New 2-Halo-2-(1H-tetrazol-5-yl)-2H-azirines via a Non-Classical Wittig Reaction" @default.
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• W2196237611 doi "https://doi.org/10.3390/molecules201219848" @default.
• W2196237611 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/6332326" @default.
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• W2196237611 hasPublicationYear "2015" @default.
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